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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 179, 2004 - Issue 8
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Original Articles

TRIFLUOROMETHYLTHIOCOPPER CATALYZED OXIRANE RING OPENING

S. Munavalli Geo-Centers, Inc., APG, Edgewood, Maryland, USA
,
D. K. Rohrbaugh U.S. Army, Edgewood Chemical and Biological Center, Aberdeen Proving Ground, Edgewood, Maryland, USA
&
H. D. Durst U.S. Army, Edgewood Chemical and Biological Center, Aberdeen Proving Ground, Edgewood, Maryland, USA
Pages 1657-1671 | Received 01 Nov 2003, Accepted 01 Dec 2003, Published online: 16 Aug 2010
 
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Abstract

Trifluoromethylthiocopper has been found to catalyze the opening of the epoxide ring and to furnish not-so-easily accessible novel trifluoromethylthiolated α-hydroxy compounds. This communication presents the mechanism of the formation of the various compounds and their mass spectral data.

Notes

∗Ellute close together and could not be separated; combined yields 19.8%.

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