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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 179, 2004 - Issue 11
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Original Articles

ALANINE/CHLOROCHROMIC ACID/SILICA GEL: AN EFFICIENT AND SELECTIVE REAGENT FOR THE OXIDATION OF ORGANIC FUNCTIONAL GROUPS

Peyman Salehi Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran;, 19835-389
,
Mohammad Mehdi Khodaei Department of Chemistry, Faculty of Science, Razi University, Kermanshah, Iran
&
Amin Rostami Department of Chemistry, Faculty of Science, Razi University, Kermanshah, Iran
Pages 2235-2243 | Received 01 Mar 2004, Published online: 16 Aug 2010
 
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Abstract

Alanine/chlorochromic acid/silica gel is a new and selective reagent for the efficient oxidation of sulfides, thiols, oximes, and alcohols. Oxidation of sulfides is solvent dependent. In chloroform at room temperature sulfoxides are formed as the major products, while in carbon tetrachloride or under solvent-free conditions solfones are produced in good-to-excellent yields.

Notes

a Sulfoxides were produced as the final products.

b Sulfones were produced as the final products.

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