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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 179, 2004 - Issue 12
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Original Articles

SYNTHESIS OF MONO-AND DIALKYLPHOSPHATES BY THE REACTIONS OF HYDROXYCOMPOUNDS WITH THE PHOSPHORUS PENTAOXIDE UNDER MICROWAVE IRRADIATION

Abdelhamid Elias Organic Synthesis Laboratory, CRND, Draria, Algers, Algeria
,
M. Amine Didi Catalysis Laboratory, Chemistry Department, Tlemcen University, Algeria
,
Didier Villemin LCMT, ENSICAEN, Caen University, Caen, France
,
T. Semaoune Organic Synthesis Laboratory, CRND, Draria, Algers, Algeria
&
S. Ouattas Organic Synthesis Laboratory, CRND, Draria, Algers, Algeria
Pages 2599-2607 | Received 01 May 2004, Accepted 01 May 2004, Published online: 16 Aug 2010
 
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Abstract

The reactions of phosphorus pentoxide with two alcohols and one phenol were performed in different conditions under microwave irradiation. The products (alkylphosphates and dialkylphosphates) were identical to those formed by classic heating and were obtained with better yields. The speed of the reaction was increased by a factor from 100 to 4000.

Notes

* δ, chemical shift; ν, wave number; s, singulet; d, doublet; t, triplet; q, quadruplet; quint, quintuplet; sext, sextuplet; m, multiplet; J, coupling constante; S, strong; L, large; w, weak.

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