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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 183, 2007 - Issue 1
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Original Articles

Facile Solvent-Free Generation of Disulfide Dianion and its Use for Preparation of Symmetrical Disulfides

Ali Reza Kiasat Chemistry Department, College of Sciences, Shahid Chamran University, Ahwaz, Iran
,
Babak Mokhtari Chemistry Department, College of Sciences, Shahid Chamran University, Ahwaz, Iran
,
Ali Savari Chemistry Department, College of Sciences, Shahid Chamran University, Ahwaz, Iran
&
Foad Kazemi Department of Chemistry, Institute for Advanced Studies in Basic Sciences (IASBS), Gava Zang, Zanjan, Iran
Pages 178-182 | Received 27 Apr 2007, Accepted 11 Jul 2007, Published online: 20 Feb 2008
 
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Abstract

A variety of symmetrical dialkyl disulfides were prepared from the reaction of alkyl halides, sodium hydroxide and elemental sulfur under solvent free conditions. The reaction proceeded very fast and produced the desired products in moderate to excellent isolated yields.

Acknowledgments

We are thankful to the Shahid Chamran University Research Council for partial support of this work.

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