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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 183, 2008 - Issue 2-3
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Original Articles

Synthesis and Characterization of Novel Bile Acids Derived H-Phosphonates Conjugates

Yan Li Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, Tsinghua University, Beijing, P. R. China
,
Yong Ju Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, Tsinghua University, Beijing, P. R. China
&
Yufen Zhao Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, Tsinghua University, Beijing, P. R. China
Pages 706-711 | Published online: 20 Jun 2008
 
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Abstract

The H-phosphnates of bile acid, conjugated with several alcohols and nucleosides, were synthesized in one pot by a tandem transesterification with diphenyl phosphate. The structures of these novel bile acid conjugates were confirmed by IR, 31P NMR, 1H NMR and HRMS.

Acknowledgments

Project supported by the NSF of China (No. 20772071) and SRFDP of Higher Education (No. 20050003104).

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