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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 183, 2008 - Issue 2-3
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Original Articles

Novel Benzo-and Pyrido-Anellated 1, 3-Azaphospholes

J. Heinicke Institut für Biochemie-Anorganische Chemie, Universität Greifswald, Greifswald, Germany
,
B. R. Aluri Institut für Biochemie-Anorganische Chemie, Universität Greifswald, Greifswald, Germany
,
M. S.S. Adam Institut für Biochemie-Anorganische Chemie, Universität Greifswald, Greifswald, Germany
&
P. G. Jones Institut füur Anorganische und Analytische Chemie, Technische Universität Braunschweig, Braunschweig, Germany
Pages 779-782 | Published online: 20 Jun 2008
 
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Abstract

We present the synthesis of OH-functional and bulky N-substituted benzazaphospholes, novel pyrido-azaphospholes, addition versus CH-metalation by tBuLi and reactions with electrophiles yielding a novel asymmetric P,N-heterocyclic ethylene-1,2-bis(phosphine) and phosphino-functional benzazaphospholes for hemilabile σ3,σ2–P,P′ coordination.

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