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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 183, 2008 - Issue 9
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Original Articles

A Low-Temperature Route for ReP2O7 Synthesis

V. V. Lisnyak Chemical Department, Kyiv National T. Shevchenko University, Kyiv, Ukraine
,
N. V. Stus Chemical Department, Kyiv National T. Shevchenko University, Kyiv, Ukraine
,
D. A. Stratiichuk Institute for Superhard Materials, the National Academy of Science of Ukraine, Kyiv, Ukraine
,
N. M. Belyavina Physical Department, Kyiv National T. Shevchenko University, Kyiv, Ukraine
&
V. Ya. Markiv Physical Department, Kyiv National T. Shevchenko University, Kyiv, Ukraine
Pages 2248-2255 | Received 15 Dec 2007, Accepted 11 Jan 2008, Published online: 12 Aug 2008
 
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Abstract

A low-temperature route for the synthesis of the Re(IV) diphosphate starting from ReO4 − is presented. The ReP2O7 polycrystals have been prepared in 63% yield by an interaction of NH4ReO4 with molten phosphoric acid at 673 K with subsequent cooling down to 298 K. The synthesized ReP2O7 was characterized by X-ray powder diffraction (XRPD) and DRIFT spectroscopy.

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