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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 184, 2009 - Issue 12
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Original Articles

Catalytic Performance of Divanadium-Substituted Molybdophosphate Acid, H5PMo10V2O40, in Liquid-Phase Esterification of Hexanoic Acid

Fatemeh F. Bamoharram Department of Chemistry, Islamic Azad University–Mashhad Branch, Mashhad, Iran
,
Majid M. Heravi Department of Chemistry, School of Sciences, Azzahra University, Vanak, Tehran, Iran
,
Mina Roshani Department of Chemistry, Islamic Azad University–Mashhad Branch, Mashhad, Iran
&
Hamzeh Mir Department of Chemistry, Islamic Azad University–Mashhad Branch, Mashhad, Iran
Pages 3119-3125 | Received 08 Jul 2008, Accepted 10 Nov 2008, Published online: 18 Nov 2009
 
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Abstract

Divanadium-substituted molybdophosphate acid, H5PMo10V2O40, efficiently catalyzes the synthesis of ethylhexanoate from hexanoic acid and ethanol at reflux temperature and under solventless conditions. Comparison of H5PMo10V2O40 with the other heteropolyacids showed that this catalyst gives the highest total yield of ethylhexanoate. The effects of the molar ratio of acid:alcohol, reaction times, and temperatures were studied.

Notes

a Yields determined by GC/MS.

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