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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 184, 2009 - Issue 5: Honoring the 70th Birthday of Marian Mikolajczyk, Part 2
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Original Articles

Synthesis and Structure Determination of Some Monothio- and Dithioimides Derived from Succinic and Glutaric Acids

Michał Pawłowski Faculty of Chemistry, Warsaw University, Warsaw, Poland
,
Anna Lendzion Faculty of Chemistry, Warsaw University, Warsaw, Poland
,
Joanna Szawkało Faculty of Chemistry, Warsaw University, Warsaw, Poland
,
Andrzej Leniewski Faculty of Chemistry, Warsaw University, Warsaw, Poland
,
Jan K. Maurin National Medicines Institute, Warsaw, Poland; Institute of Atomic Energy, Otwock-Świerk, Poland
&
Zbigniew Czarnocki Faculty of Chemistry, Warsaw University, Warsaw, Poland
Pages 1307-1313 | Received 14 Jan 2008, Accepted 29 Jan 2008, Published online: 28 Apr 2009
 
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Abstract

A series of novel 5-thioxopyrrolidin-2-ones and 6-thioxopiperidin-2-ones was synthesized using Lawesson's reagent in thionation of the appropriate imides. The NMR data were determined, and in one case the structure assignment was additionally supported by X-ray crystallography.

Dedicated to Professor Marian Mikołajczyk, CBMiM PAN in Łódź, Poland, on the occasion of his 70th birthday.

Financial support from grants PBZ-KBN-126/T09/2004/13 and 501/68-BW-175610 is gratefully acknowledged.

Notes

$ Satisfactory microanalyses were obtained for all compounds: C ± 0.22, H ± 0.08, N ± 0.08, S ± 0.14%.

# Exchangeable with D2O.

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