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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 185, 2010 - Issue 4
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Original Articles

Monitoring the Phosphorylation of Phenol with Diethyl Chlorophosphate in Aqueous Medium in the Presence of Sodium Hydroxide by in Situ Fourier Transform Infrared Spectroscopy

György Keglevich Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Réka Eszter Puskás Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Alajos Grün Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary; Research Group of the Hungarian Academy of Sciences at the Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
&
István Csontos Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
Pages 832-837 | Received 20 Mar 2009, Accepted 27 Apr 2009, Published online: 23 Mar 2010
 
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Abstract

In situ Fourier transform IR spectroscopy has been found to be an appropriate tool for monitoring the title reaction resulting in the formation of diethyl phenylphosphate.

Acknowledgments

The authors are grateful for the OTKA (T067679) support of this work.

Notes

a Shoulder.

b A broad signal results from νP˭O/νP–O–C (aryl) vibrations.

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