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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 185, 2010 - Issue 4
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Original Articles

Addition of Hypophosphorous Acid to N,N′-Terephthalylidene-bis[1-(alkoxycarbonyl)alkylamines]

Jarosław Lewkowski Department of Organic Chemistry, University of Łódź, Łódź, Poland
&
Marek Dzięgielewski Department of Organic Chemistry, University of Łódź, Łódź, Poland
Pages 838-841 | Received 23 Mar 2009, Accepted 27 Apr 2009, Published online: 23 Mar 2010
 
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Abstract

The preparation of 1,4-phenylene-bis[1-(alkoxycarbonyl)alkylamino-methanephosphonous acids] by the addition of hypophosphorous acid to terephthalylidene-bis[1-(alkoxycar bonyl)alkylamines] is described. Despite expectations, no chiral assistance of the amino acid ester moiety is observed.

Acknowledgments

Financial support of the Polish Ministry of Science and Higher Education is kindly acknowledged.

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