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Original Articles

Efficient One-Pot Synthesis of Naphthoquinone-Fused Phosphorous Heterocycles via Mannich-Type Reaction

, &
Pages 2739-2748 | Received 26 Mar 2009, Accepted 03 Jun 2009, Published online: 21 Sep 2009
 

Abstract

A series of naphthoquinone-fused phosphorus heterocycles was synthesized via a three-component Mannich-type reaction. 2-Chloroethoxylphosphorodichloridite was used as a phosphorus substrate to explore the structure–activity relationships of the 2-position of the heterocycles. One spiral heterocycle compound was structurally characterized by a single-crystal X-ray diffraction analysis.

This work was supported by Tianjin Natural Science Foundation (Grant No. 09JCYBJC09200) and The National Basic Research Program of China (973 Program, Grant No. 2007CB914803).

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