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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 185, 2010 - Issue 8
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Original Articles

Efficient, Simple Synthesis of Stable Phosphorus Ylides Derived from 4-Aryl Urazoles

Mehdi Adib School of Chemistry, University College of Science, University of Tehran, Tehran, Iran
,
Moharram Omidi School of Chemistry, University College of Science, University of Tehran, Tehran, Iran
&
Hamid Reza Bijanzadeh Department of Chemistry, Tarbiat Modarres University, Tehran, Iran
Pages 1732-1738 | Received 09 Jun 2009, Accepted 11 Aug 2009, Published online: 02 Aug 2010
 
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Abstract

Crystalline phosphorus ylides are obtained in nearly quantitative yields from the 1:1:1 addition reaction between triphenylphosphine, dialkyl acetylenedicarboxylates, and 4-aryl urazoles.

Acknowledgments

This research was supported by the Research Council of the University of Tehran as a research project (6102036/1/03).

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