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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 185, 2010 - Issue 11
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Original Articles

Monitoring the Phosphorylation of Phenol Derivatives with Diethyl Chlorophosphate in Liquid–Liquid and Solid–Liquid Phase by In Situ Fourier Transform Infrared Spectroscopy, Part II

György Keglevich Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Réka Eszter Puskás Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Alajos Grün Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary; Research Group of the Hungarian Academy of Sciences at the Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
István Csontos Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
&
István Greiner Gedeon Richter Plc., Budapest, Hungary
Pages 2333-2340 | Received 04 Dec 2009, Accepted 11 Jan 2010, Published online: 05 Nov 2010
 
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Abstract

The reaction of 4-chlorophenol and 4-nitrophenol with diethyl chlorophosphate carried out in a liquid–liquid and solid–liquid two phase system, respectively, was monitored by in situ Fourier transform IR spectroscopy.

Acknowledgments

The authors are grateful for the OTKA (K067679) support of this work.

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