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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 185, 2010 - Issue 5-6: A Tribute to the Chemistry of Professor Naomichi Furukawa
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Original Articles

Preparation of Octakis (methylthio)octaethylphthalocyaninato Titanium (IV) Benzenedichalcogenolates

Takeshi Kimura Center for Instrumental Analysis, Iwate University, Iwate, Japan
,
Arata Yamamoto Center for Instrumental Analysis, Iwate University, Iwate, Japan
&
Toshiharu Namauo Center for Instrumental Analysis, Iwate University, Iwate, Japan
Pages 1008-1013 | Received 26 Nov 2008, Accepted 17 Dec 2008, Published online: 27 May 2010
 
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Abstract

Octakis(methylthio)octaethylphthalocyaninato titanium (IV) oxide (PcSMeTiO) was prepared from octakis(methylthio)octaethylphthalocyanine (PcSMe) upon treatment with titanium (IV) tetrabutoxide in DMF at 130°C. The reaction of PcSMeTiO with benzenedithiol or benzenediselenol produced octakis(methylthio)octaethylphthalocyaninato titanium (IV) benzenedichalcogenolates (4a,b) bearing titanium–sulfur or titanium–selenium bonds.

Acknowledgments

Dedicated to Professor Naomichi Furukawa on the occasion of his 70th birthday.

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