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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 2
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Regular Articles

Preparation of α-Ketophosphonate Derivatives and Their Application in the Synthesis of 1-(N-Alkylcarbamoyl)-1-(diethoxyphosphoryl)alkyl Benzoates via Passerini Reaction

Javad AzizianChemistry Department, Science and Research Branch, Islamic Azad University, Tehran, Iran
,
Ali RamazaniChemistry Department, Islamic Azad University–Zanjan Branch, Zanjan, Iran
&
Mohammad HajiChemistry Department, Science and Research Branch, Islamic Azad University, Tehran, Iran
Pages 326-333 | Received 12 Mar 2010, Accepted 22 May 2010, Published online: 19 Feb 2011
 
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Abstract

The Passerini reaction of α-ketophosphonates, isocyanides, and benzoic acid derivatives leads to 1-(N-alkylcarbamoyl)-1-(diethoxyphosphoryl)alkyl benzoates in one step at room temperature. The structures of products were assigned on the basis of their 1H NMR, 13C NMR, 31P NMR, and IR spectroscopic data.

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