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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 4: 18th International Conference on Phosphorus Chemistry (ICPC2010)
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I. Synthesis and Applications in Catalysis

Tetrakis(trimethylsilyl) Ethenylidenebisphosphonate: A Mild and Useful Reagent for the Synthesis of Substituted 2-Aminoethylidene-1,1-bisphosphonic Acids

Michael V. Shevchuk Taras Shevchenko National University of Kyiv, Department of Organic Chemistry, Kyiv, Ukraine
,
Vadim D. Romanenko Institute of Bioorganic Chemistry and Petrochemistry, Department of Fine Organic Synthesis, Kyiv, Ukraine
&
Valery P. Kukhar Institute of Bioorganic Chemistry and Petrochemistry, Department of Fine Organic Synthesis, Kyiv, Ukraine
Pages 799-801 | Received 09 Apr 2010, Accepted 01 Jun 2010, Published online: 25 Apr 2011
 
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Abstract

Tetrakis(trimethylsilyl) ethenylidenebisphosphonate is proposed as a substrate in the preparations of N-substituted 2-aminoethylidene-1,1-bisphosphonic acids. The method provides an extremely mild protocol for the synthesis of these compounds and is compatible with a wide range of functional groups.

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