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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 4: 18th International Conference on Phosphorus Chemistry (ICPC2010)
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I. Synthesis and Applications in Catalysis

3,3-Bis(diethylphosphono)-1(3H)-isobenzofuranone and Its Properties

V. N. Zemlianoy Institute of Bioorganic Chemistry and Petroсhemistry, National Academy of Sciences of Ukraine, Kyiv, Ukraine
,
A. O. Kolodiazhna Institute of Bioorganic Chemistry and Petroсhemistry, National Academy of Sciences of Ukraine, Kyiv, Ukraine
,
A. V. Gutov Institute of Bioorganic Chemistry and Petroсhemistry, National Academy of Sciences of Ukraine, Kyiv, Ukraine
,
A. N. Chernega Institute of Bioorganic Chemistry and Petroсhemistry, National Academy of Sciences of Ukraine, Kyiv, Ukraine
,
V. P. Kukhar Institute of Bioorganic Chemistry and Petroсhemistry, National Academy of Sciences of Ukraine, Kyiv, Ukraine
&
O. I. Kolodiazhnyi Institute of Bioorganic Chemistry and Petroсhemistry, National Academy of Sciences of Ukraine, Kyiv, Ukraine
Pages 772-774 | Received 07 Jul 2010, Accepted 08 Jul 2010, Published online: 25 Apr 2011
 
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Abstract

The reaction of o-phthaloyl chloride with sodium diethylphosphite led to the formation of new 3,3-bis(diethylphosphono)-1-(3H)-isobenzofurane 1. The reaction of bis-phosphonate with alkylamine occurs with replacement of an ester oxygen by an imine group to afford the crystalline isoindolyl-bis-phosphonate—a representative of this new type of organophosphorus heterocycles.

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