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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 4: 18th International Conference on Phosphorus Chemistry (ICPC2010)
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II. Theoretical and Structural Chemistry

New Method for the Preparation of Octathiotetraphosphetanes on the Basis of Elemental Phosphorus and Sulfur: Structure and Properties

Oleg G. Sinyashin A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
,
Elvira S. Batyeva A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
,
Valery I. Kovalenko A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
,
Elena K. Badeeva A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
,
Elena V. Platova A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
,
Alexander E. Vandyukov A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
,
Elena E. Zvereva A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
&
Lidiya I. Kursheva A. E. Arbuzov Institute of Organic & Physical Chemistry of RAS, Kazan, Russia
 show all
Pages 852-853 | Received 21 Jul 2010, Accepted 04 Aug 2010, Published online: 25 Apr 2011
 
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Abstract

New octathiotetraphosphetane ammonium salts are obtained based on the reaction of white phosphorus (Р4) and elemental sulfur with aliphatic mercaptans in the presence of amines (morpholine, methylmorpholine, pyrrolidine, and N,N-dimethylbenzylamine). The salts of octathiotetraphosphetane are characterized by IR/Raman spectroscopy. Several common IR and Raman bands can be used as structural markers for establishing the structures of [P4S8]4− anion in new compounds.

Acknowledgments

Financial support from the Russian Foundation for Basic Research (grant no. 09-03-00006-a) is gratefully acknowledged.

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