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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 5: 24th International Symposium on the Organic Chemistry of Sulfur
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Oral Contributions

Synthesis of Novel Highly Soluble N-(3,5-Di-tert-butylbenzyl)-monopyrrolo-tetrathiafulvalene Derivatives

Mr Andreas Denhof Department of Chemistry, University of Bremen, Bremen, Germany
,
Mr Jens Cordes Department of Chemistry, University of Bremen, Bremen, Germany
&
Dr Vladimir A. Azov Department of Chemistry, University of Bremen, Bremen, Germany
Pages 1278-1283 | Received 24 Jun 2010, Accepted 13 Sep 2010, Published online: 12 Jul 2011
 
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Abstract

Highly soluble bis-(2-cyanoethyl)-protected derivative (11) of monopyrrolo-tetrathiafulvalene containing a bulky 3,5-di-tert-butylbenzyl solubilizing group has been synthesized and characterized. It was successfully employed to prepare two aromatic conjugates of monopyrrolo-tetrathiafulvalenes (TTFs) and is proposed to be used for preparation of TTF-containing molecular tweezers.

Acknowledgments

We are grateful to Dr. T. Dülcks and D. Kemken for recording MS spectra.

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