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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 4: 18th International Conference on Phosphorus Chemistry (ICPC2010)
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IV. Biologically Relevant Organophosphorus Compounds

Synthesis and Sensing of Bisphosphonophosphate Alkyl Monoesters: A Novel Class of Compounds for the Study of Nucleoside 5′-Triphosphate Chemistry

Brian T. Chamberlain Department of Chemistry, University of Southern California, Los Angeles, California, USA
,
Jorge Osuna Department of Chemistry, University of Southern California, Los Angeles, California, USA
,
Boris A. Kashemirov Department of Chemistry, University of Southern California, Los Angeles, California, USA
&
Charles E. McKenna Department of Chemistry, University of Southern California, Los Angeles, California, USA
Pages 966-967 | Received 16 Sep 2010, Accepted 21 Sep 2010, Published online: 25 Apr 2011
 
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Abstract

A series of novel β,γ-methylene-, monofluoromethylene-, and difluoromethylene-bisphosphonophosphate alkyl monoesters was synthesized. The compounds were conveniently detected during preparative HPLC using post-column derivatization with a phosphate-specific chemosensor.

Acknowledgments

This work was supported by the Intramural Research Program of the NIH, National Institute of Environmental Health Sciences, and by NIH program project grant 5-U19-CA105010.

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