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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 4: 18th International Conference on Phosphorus Chemistry (ICPC2010)
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I. Synthesis and Applications in Catalysis

Synthesis of Phosphinic Acid Pseudodipeptides of C2-Symmetry

Babak Kaboudin Department of Chemistry, Institute for Advanced Studies in Basic Sciences, Gava Zang, Zanjan, Iran
,
Fariba Saadati Department of Chemistry, Institute for Advanced Studies in Basic Sciences, Gava Zang, Zanjan, Iran
&
Tsutumo Yokomatsu School of Pharmacy, Tokyo University of Pharmacy and Life Sciences, Tokyo, Japan
Pages 804-805 | Received 16 Sep 2010, Accepted 20 Sep 2010, Published online: 25 Apr 2011
 
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Abstract

Treatment of aromatic aldehydes with ammonia and hypophosphorus acid gave C 2-symmetric 1-aminoarylmethylphosphinic acids. The latter compounds, activated in the presence of hexamethyldisilazane (HMDS) or trimethylsilyl chloride (TMSCl), successfully reacted with methyl acrylate to afford symmetric pseudodipeptides. The applied synthetic approach is briefly outlined here.

Acknowledgments

The authors gratefully acknowledge support by the Institute for Advanced Studies in Basic Sciences (IASBS) Research Council under grant No. G2009IASBS120.

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