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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 9
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Original Articles

Synthesis of Dialkyl Phosphorylsuccinates from the Reaction of Thiouracil Derivatives with Dialkyl Acetylenedicarboxylates in the Presence of Trialkylphosphites

Javad AzizianDepartment of Chemistry, Science and Research Branch, Islamic Azad University, Ponak, Tehran, Iran
,
Khadijeh YadollahzadehDepartment of Chemistry, Science and Research Branch, Islamic Azad University, Ponak, Tehran, Iran
,
Hasan TahermansouriDepartment of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, Amol, Iran
&
Akram Sadat DelbariDepartment of Chemistry, Islamshahr Branch, Islamic Azad University, Islamshar, Iran
Pages 1844-1852 | Received 27 Sep 2010, Accepted 26 Nov 2010, Published online: 24 Aug 2011
 
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Abstract

Dialkyl-2-(dialkoxyphosphonyl)-3-(1,6-dihydro-6-oxo-4-propylpyrimidin-2-ylthio) succinates and dialkyl-2-(dialkoxyphosphonyl)-3-(1,6-dihydro-6-oxopyrimidin-2-ylthio) succinates were synthesized in moderate to high yields using a novel, facile, and one-pot condensation of dialkyl acetylenedicarboxylates, trialkylphosphites, and thiouracil derivatives.

Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the free supplemental file.

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