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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 187, 2012 - Issue 6
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Original Articles

Efficient α-Thiocyanation of Ketones Using Pyridinium Hydrobromide Perbromide

Liqiang Wu School of Pharmacy, Xinxiang Medical University, Xinxiang, Henan, China
&
Xiaojuan Yang College of Chemistry and Chemical Engineering, Xinxiang University, Xinxiang, Henan, China
Pages 748-753 | Received 31 May 2011, Accepted 18 Aug 2011, Published online: 05 Apr 2012
 
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Abstract

The direct α-thiocyanation of ketones with ammonium thiocyanate has been achieved using pyridinium hydrobromide perbromide under mild and neutral conditions to produce α-ketothiocyanates in excellent yields and with high selectivity.

GRAPHICAL ABSTRACT

Acknowledgments

We are pleased to acknowledge the financial support from Xinxiang Medical University.

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