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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 187, 2012 - Issue 5
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Original Articles

A New Method of Introducing SCH3 and SCD3 Groups to Phosphorothioates

Tianzhen Liu Department of Chemistry, College of Science, Tianjin University, Tianjin, China
,
Xiaoxue Cui Department of Chemistry, College of Science, Tianjin University, Tianjin, China
,
Zhifang Yu Department of Chemistry, College of Science, Tianjin University, Tianjin, China
&
Chunbao Li Department of Chemistry, College of Science, Tianjin University, Tianjin, China
Pages 606-611 | Received 24 Sep 2011, Accepted 17 Oct 2011, Published online: 27 Mar 2012
 
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Abstract

A new synthesis of phosphorothioates starting from phosphites and cyanuric chloride (TCT)-activated DMSO is reported herein. This method enables the incorporation of SCH3 and SCD3 groups into phosphorothioates in good yields. The labeling purities of the products are excellent.

GRAPHICAL ABSTRACT

Acknowledgments

We thank NSFC for financial support.

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