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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 188, 2013 - Issue 6
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Original Articles

Efficient Synthesis of Modified Sulfamides and Cyclosulfamides Containing Phosphonate Moieties

Sihem Hessainia Laboratory of Applied Organic Chemistry, Badji-Mokhtar Annaba University, BP 12 El-Hadjar, Annaba, Algeria
,
Malika Berredjem Laboratory of Applied Organic Chemistry, Badji-Mokhtar Annaba University, BP 12 El-Hadjar, Annaba, Algeria
,
Souad Ouarna Laboratory of Applied Organic Chemistry, Badji-Mokhtar Annaba University, BP 12 El-Hadjar, Annaba, Algeria
,
Zinelaabidine Cheraiet Laboratory of Applied Organic Chemistry, Badji-Mokhtar Annaba University, BP 12 El-Hadjar, Annaba, Algeria
&
Nour-Eddine Aouf Laboratory of Applied Organic Chemistry, Badji-Mokhtar Annaba University, BP 12 El-Hadjar, Annaba, Algeria
Pages 719-725 | Received 01 Apr 2012, Accepted 30 May 2012, Published online: 31 May 2013
 
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Abstract

The synthesis of two new series of functionalized phosphonates is described. A new entry for the synthesis of 5-phosphonoalkyl cyclosulfamides and bis(phosphonoalkyl) sulfamides starting from dihalogeno bis(amino) sulfone has been developed. These compounds have been synthesized in good yields. Triethylphosphite has been used to introduce the phosphonate moiety into sulfamides and cyclosulfamides via Arbuzov reaction.

GRAPHICAL ABSTRACT

Acknowledgments

This work was generously supported by the Direction Generale de la Recherche Scientifique et du Développement Technologique (DGRS-DT), Algerian Ministry of Scientific Research, FNR, and CMEP 08 MDU 729.

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