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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 187, 2012 - Issue 11
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Original Articles

Synthesis, Characterization, and Structures of Tetrakis(2-Pyridyl)Tin Compounds

Martin Bette Institute of Chemistry–Inorganic Chemistry, Martin Luther University of Halle-Wittenberg, Halle, Germany
&
Dirk Steinborn Institute of Chemistry–Inorganic Chemistry, Martin Luther University of Halle-Wittenberg, Halle, Germany
Pages 1271-1277 | Received 15 Mar 2012, Accepted 23 May 2012, Published online: 06 Aug 2012
 
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Abstract

Reactions of 2-bromopyridine and 2-bromo-6-methylpyridine with n-BuLi and tin tetrachloride afforded Sn(2-py)4 (1a) and Sn(6-Me-2-py)4 (1b), respectively. The identities of the two compounds were unambiguously proved by microanalyses, NMR (1H, 13C, 119Sn) spetroscopy, and single-crystal X-ray diffraction studies.

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