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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 188, 2013 - Issue 1-3: 19th International Conference on Phosphorus Chemistry (ICPC-2012) Rotterdam, 8–12 July, 2012
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Original Articles

Synthesis and Properties of Novel Calix[4]Resorcinols Containing Phosphonium Substituents

Liudmila K. Kibardina State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
,
Irina R. Knyazeva State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
,
Victoria I. Sokolova State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
,
Guzalia I. Vagapova State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
,
Lucia Ya. Zakharova State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
,
Alexander R. Burilov State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
&
Michael A. Pudovik State Budgetary-Funded Institution of Science A. E. Arbuzov Institute of Organic and Physical Chemistry of Kazan Scientific Center of Russian Academy of Sciences, Kazan, Russian Federation
 show all
Pages 1-3 | Received 16 Jul 2012, Accepted 02 Nov 2012, Published online: 08 May 2013
 
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Abstract

Condensation of resorcinol and its derivatives with novel phosphonium-substituted acetals under conditions of acidic catalysis yields either calix[4]resorcinols containing four phosphonium fragments or phosphonium salts including diarylmethane moiety depending on the structure of the phosphorus-containing reagent. The latter, in turn, undergo condensation with propionic aldehyde forming new calix[4]resorcinols with alternating phosphonium and ethyl substituents, which have remarkable surface-active properties.

GRAPHICAL ABSTRACT

Acknowledgments

The work was supported by Russian Foundation for Basic Research (grant 11-03-00416).

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