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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 189, 2014 - Issue 6
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Original Article

Convenient Synthesis of 1-(Trimethylsilyl)- and 1-(Trimethylstannyl)vinylphosphonates

Yoshiharu OkadaDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, JapanCorrespondence[email protected]
,
Tomohiro MaruyamaDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
,
Shin-ichi TamuraDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
,
Hirohito KameokaDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
,
Satoshi MasudaDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
,
Yuichiro TokudaDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
,
Junya SakaiDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
&
Masato NomuraDepartment of Biotechnology and Chemistry, Faculty of Engineering, Kinki University, Umenobe 1, Takaya, 739-2116, Higashi-Hiroshima, Japan
 show all
Pages 778-790 | Received 29 Apr 2013, Accepted 21 Sep 2013, Published online: 12 Jun 2014
 
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Abstract

Dimethyl 1,1-bis(trimethylsilyl)methylphosphonate and dimethyl 1-(trimethylsilyl)-1-(trimethylstannyl)methylphosphonate were succeeded to react with aromatic aldehydes in the presence of methyl benzoate as additive to give the corresponding vinylphosphonates in moderate yields.

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