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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 189, 2014 - Issue 7-8: Special Issue Dedicated to Louis D. Quin
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Original Articles

Synthesis and Coordination Properties of Tripodal Ligand on the Triphenylphosphine Oxide Platform with Carbamoyl Side ArmsFootnote

Igor Yu. KudryavtsevNesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow119991, RussiaCorrespondence[email protected]
,
Tat’yana V. BaulinaNesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow119991, Russia
,
Margarita P. PasechnikNesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow119991, Russia
,
Sergei V. MatveevNesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow119991, Russia
&
Anna G. MatveevaNesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow119991, Russia
Pages 946-962 | Received 02 Feb 2014, Accepted 05 Mar 2014, Published online: 04 Aug 2014
 
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Abstract

A new tripodal O-donor ligand, tris(2-N,N-dibutylcarbamoylmethoxyphenyl)phosphine oxide (L), was synthesized. This potentially tetradentate ligand L exhibits variable denticity upon complexation with UO2(NO3)2, Nd(NO3)3, and Lu(NO3)3. The complexes were studied by elemental analysis, IR, and 1H, 13C, and 31P NMR spectroscopy.

[Supplementary materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements for the following free supplemental files: Additional text, tables, and figures.]

GRAPHICAL ABSTRACT

Notes

1 This paper is dedicated to Professor Emeritus D. Louis D. Quin on the occasion of his 86th birthday.

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