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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 190, 2015 - Issue 1
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Original Articles

Convenient Synthesis of Novel N-Acylsulfonamides Containing Phosphonate Moiety

Wahida BoufasLaboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Badji-Mokhtar. Annaba University, Box 12, 23000Annaba, Algeria
,
Hadjer CheloufiLaboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Badji-Mokhtar. Annaba University, Box 12, 23000Annaba, Algeria
,
Fouzia BoucharebLaboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Badji-Mokhtar. Annaba University, Box 12, 23000Annaba, Algeria
,
Malika BerredjemLaboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Badji-Mokhtar. Annaba University, Box 12, 23000Annaba, AlgeriaCorrespondence[email protected]
&
Nour-Eddine AoufLaboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Badji-Mokhtar. Annaba University, Box 12, 23000Annaba, Algeria
Pages 103-111 | Received 12 Feb 2014, Accepted 30 May 2014, Published online: 31 Dec 2014
 
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GRAPHICAL ABSTRACT

Abstract

The present study describes a convenient method for the synthesis of new N-acylsulfonamides containing phosphonate moiety. The N-acylsulfonamides were prepared starting from chlorosulfonyl isocyanate (CSI) in four steps (carbamoylation, sulfamoylation, deprotection, and acylation). Trimethylphosphite has been used to introduce the phosphonate moiety into N-acylsulfonamides via Arbuzov reaction.

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