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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 190, 2015 - Issue 7
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Original Articles

AlCl3-Promoted Thiocyanation of N-Containing Aromatic and Heteroaromatic Compounds Under Solvent-Free Conditions

Kobra NikoofarDepartment of Chemistry, Faculty of Science, Alzahra University, Vanak, Tehran, IranCorrespondence[email protected] [email protected]
&
Samareh GorjiDepartment of Chemistry, Faculty of Science, Alzahra University, Vanak, Tehran, Iran
Pages 1138-1145 | Received 23 Jun 2014, Accepted 14 Oct 2014, Published online: 25 Jul 2015
 
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GRAPHICAL ABSTRACT

Abstract

Aluminum chloride/Ammonium thiocyanate (AlCl3/NH4SCN) was found to be an effective system for the thiocyanation of some arylamines and indoles to afford the corresponding thiocyanated adducts at room temperature under solvent-free conditions. The efficacy of this combined reagent was also examined in the thiocyanation of pyrrole and isatin. A plausible mechanism of thiocyanation has also been suggested.

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