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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 190, 2015 - Issue 5-6: 20th International Conference on Phosphorus Chemistry (ICPC-2014)
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Original Articles

PPN Pyrophosphate: A New Reagent for the Preparation of Nucleoside Triphosphates

Heidi J. KorhonenDepartment of Chemistry, University of Turku, Finland;Department of Chemistry and Biophysical Sciences Institute, Science Laboratories, Durham University, South Road, Durham, United Kingdom
,
Hannah L. BoltDepartment of Chemistry and Biophysical Sciences Institute, Science Laboratories, Durham University, South Road, Durham, United Kingdom
,
Leyre Vicente-GinesDepartment of Chemistry and Biophysical Sciences Institute, Science Laboratories, Durham University, South Road, Durham, United Kingdom
,
Daniel C. PerksDepartment of Chemistry and Biophysical Sciences Institute, Science Laboratories, Durham University, South Road, Durham, United Kingdom
&
David R. W. HodgsonDepartment of Chemistry and Biophysical Sciences Institute, Science Laboratories, Durham University, South Road, Durham, United KingdomCorrespondence[email protected]
Pages 758-762 | Received 31 Aug 2014, Accepted 30 Oct 2014, Published online: 01 Jul 2015
 
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GRAPHICAL ABSTRACT

Abstract

Tris{bis(triphenylphosphoranylidene) ammonium} (PPN) pyrophosphate was accessed via aqueous precipitation and desiccation. The reagent was investigated as a replacement for highly hygroscopic alkylammonium salts in Ludwig–Yoshikawa reactions for the preparation of nucleoside-5′-triphosphates.

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