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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 191, 2016 - Issue 6
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Original Articles

Three-component reactions of phosphorus ylides, thiophenols, and acetyl chloride for the synthesis of (β-thioacrylates)

Yunyun LiuKey Laboratory of Functional Small Organic Molecules, Ministry of Education, and College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, P. R. ChinaCorrespondence[email protected]
&
Bin HuangKey Laboratory of Functional Small Organic Molecules, Ministry of Education, and College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, P. R. China
Pages 926-929 | Received 07 Sep 2015, Accepted 26 Oct 2015, Published online: 28 Apr 2016
 
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GRAPHICAL ABSTRACT

ABSTRACT

The facile synthesis of β-thioacrylates has been realized via direct three-component reactions of thiophenols, Wittig reagents, and acetyl chloride. Under transition metal-free conditions, a class of β-thioacrylates have been synthesized with fair to excellent yields via cascade C=C double bond and C(spCitation2)-S bond formation.

Funding

This work is financially supported by the National Natural Science Foundation of China (21202064) and Natural Science Foundation of Jiangxi Province (20142BAB213007).

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