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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 191, 2016 - Issue 11-12: 21st International Conference on Phosphorus Chemistry (ICPC-2016)
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Original Articles

The resolution and application of P-stereogenic phosphine oxides

Péter BagiDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryCorrespondence[email protected]
,
Réka HerbayDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Kinga JuhászDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Bence VargaDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Elemér FogassyDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
&
György KeglevichDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
Pages 1459-1461 | Received 08 Jul 2016, Accepted 08 Jul 2016, Published online: 15 Jul 2016
 
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GRAPHICAL ABSTRACT

ABSTRACT

Resolution methods involving the formation of diastereomeric complexes were developed for the separation of cyclic P-stereogenic phosphine oxides and phosphinates. These resolution methods are of more general value, as they can be applied also for the enantioseparation of acyclic phosphine oxides. 5- and 6-Membered cyclic phosphine oxides were deoxygenated and then converted to platinum complexes which can be applied as catalysts in enantioselective hydroformylation.

Funding

The authors are thankful to the Hungarian Research Fund for financial support (Grant No. PD116096).

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