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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 191, 2016 - Issue 11-12: 21st International Conference on Phosphorus Chemistry (ICPC-2016)
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Original Articles

Modification of bicyclic phosphonates based on resorcinol and its derivatives via Mannich reaction

Yulia M. SadykovaA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, RussiaCorrespondence[email protected]
,
Yulia K. VoroninaA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, Russia
,
Alexander R. BurilovA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, Russia
&
Michael A. PudovikA.E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Kazan, Russia
Pages 1560-1561 | Received 12 Jul 2016, Accepted 12 Jul 2016, Published online: 05 Aug 2016
 
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GRAPHICAL ABSTRACT

ABSTRACT

Amino-containing derivatives of various structures have been obtained via Mannich reaction in a series of bicyclic phosphonates based on 2-methylresorcinol, resorcinol, and pyrogallol with paraformaldehyde and secondary amines via Mannich reaction. The structure and composition of the obtained compounds have been determined using 31P and 1H NMR spectroscopy, IR spectroscopy, mass spectrometry (MALDI-TOF), and X-ray analysis.

Funding

This work was funded by the Russian Foundation for Basic Research (grant no. 14-03-00191-a).

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