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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 192, 2017 - Issue 6: Harry Hudson Special Issue
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Original Articles

Revisiting the reaction of phosphole oxide dimers with borane-dimethylsulfide

Tamara KovácsDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Dóra CseresnyésDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
László DrahosInstitute of Organic Chemistry Research Centre for Natural Sciences Hungarian Academy of Sciences, Budapest, Hungary
&
György KeglevichDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryCorrespondence[email protected]
Pages 695-699 | Received 22 Jan 2016, Accepted 07 Jan 2017, Published online: 25 May 2017
 
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GRAPHICAL ABSTRACT

ABSTRACT

The selective reduction and boronation of the P-phenyl phosphole oxide dimer applying BH3·SMe2 as the reagent was investigated. The optimized protocol allowing the P˭O→P→BH3 conversion at 26°C in concentrated CH2Cl2 solution could be well extended also to a series of P-alkyl phosphole oxide dimers.

Funding

This project was supported by the Hungarian Research Development and Innovation Fund (K119202).

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