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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 193, 2018 - Issue 3
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Original Articles

An efficient synthesis of 2-Aminoethylidene-1,1-Bisphosphonates derivatives via Michael addition reaction

Mingxiu LvSchool of Material and Chemical Engineering, Henan University of Engineering, Zhengzhou, ChinaCorrespondence[email protected]
,
Mengwei WangSchool of Material and Chemical Engineering, Henan University of Engineering, Zhengzhou, China;College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, China
,
Kui LuSchool of Material and Chemical Engineering, Henan University of Engineering, Zhengzhou, China
,
Lu PengSchool of Material and Chemical Engineering, Henan University of Engineering, Zhengzhou, China
&
Yufen ZhaoCollege of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, China;Departmentl of Chemistry, Xiamen University, Xiamen, China
Pages 149-154 | Received 05 Jun 2017, Accepted 13 Oct 2017, Published online: 07 Nov 2017
 
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GRAPHICAL ABSTRACT

ABSTRACT

A facile, rapid and cheap synthetic strategy towards a wide range of novel 2-aminoethylidene-1,1-bisphosphonate derivatives was developed through the Michael addition reaction of various aromatic amines, aromatic amides as well as nucleoside analogues with tetraethyl ethenylidene-1,1-bisphosphonate. All the newly obtained compounds were characterized by 1H, 31P, 13C NMR spectroscopy, IR and HR MS.

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