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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 193, 2018 - Issue 4
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Original Articles

DCC-assisted direct esterification of phosphinic and phosphoric acids with O-nucleophiles

Biquan XiongDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaCorrespondence[email protected]
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,
Gang WangDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaView further author information
,
Congshan ZhouDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaView further author information
,
Yu LiuDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaView further author information
,
Jiandong LiDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaView further author information
,
Pangliang ZhangDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaView further author information
&
Kewen TangDepartment of Chemistry and Chemical Engineering, Hunan Institute of Science and Technology, Yueyang, P.R.ChinaView further author information
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Pages 239-244 | Received 24 Jul 2017, Accepted 11 Oct 2017, Published online: 13 Nov 2017
 
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GRAPHICAL ABSTRACT

ABSTRACT

A novel and efficient dicyclohexylcarbodiimide-promoted protocol for the selective and controllable esterification of P(O)OH compounds using O-nucleophiles (alcohols and phenols) as efficient esterification reagents is described. This method features a high efficiency and good functional-group tolerance, meaning a simple way to synthesize a broad spectrum of phosphinic and phosphoric acid esters from basic starting materials with moderate to excellent yields.

Acknowledgment

This work was supported by National Natural Science Foundation of China (21606080, 21676077, 21476068), Scientific Research Fund of Hunan Provincial Education Department (16B111).

Additional information

Funding

National Natural Science Foundation of China(10.13039/501100001809, 21476068, 21606080, 21676077), Scientific Research Fund of Hunan Provincial Education Department, 16B111)

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