Advanced search
Publication Cover
Phosphorus, Sulfur, and Silicon and the Related Elements Volume 194, 2019 - Issue 4-6: Proceedings of the 2018 International Conference on Phosphorus Chemistry, ICPC-22
Submit an article Journal homepage
117
Views
1
CrossRef citations to date
0
Altmetric
Short Communication

Diphenylphosphorylacetic acid thiosemicarbazide and its solvate: Single crystal X-ray analysis

A. I. SamigullinaArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, Russian Federation; Correspondence[email protected]
ORCID Iconhttp://orcid.org/0000-0002-6791-9973View further author information
ORCID Icon,
I. A. KrutovKazan National Research Technological University, Kazan, Russian FederationView further author information
,
E. L. GavrilovaKazan National Research Technological University, Kazan, Russian FederationView further author information
&
A. T. GubaidullinArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, Russian Federation; View further author information
Pages 300-301 | Received 28 Sep 2018, Accepted 19 Oct 2018, Published online: 18 Nov 2018
 
Sample our Physical Sciences journals, sign in here to start your FREE access for 14 days

Abstract

Structures of the individual compound 2-(2-(diphenylphosphoryl)acetyl)-N-phenylhydrazinecarbothioamide and its solvate with DMSO were determined by the single X-ray analysis. Despite the lability of the system, in crystals of two modifications the similar conformation of the molecule is realized. In the crystals of individual thiosemicarbazide and its solvate form 1 D supramolecular structures, but the crystal packing of them is distinguished significantly. Solvent molecules are located in the 0D-voids in the crystals.

Graphical Abstract

Additional information

Funding

The Synthetic part of work was supported by the Russian Science Foundation (project no. 14-23-00073-p), crystallographic part was supported by the Russian Foundation for Basic Research (grant No 18-33-00228).

Log in via your institution

Access through your institution

Log in to Taylor & Francis Online

Restore content access

Restore content access for purchases made as guest
Purchase options * Save for later

PDF download + Online access

  • 48 hours access to article PDF & online version
  • Article PDF can be downloaded
  • Article PDF can be printed
USD 61.00 Add to cart

Issue Purchase

  • 30 days online access to complete issue
  • Article PDFs can be downloaded
  • Article PDFs can be printed
USD 2,235.00 Add to cart

* Local tax will be added as applicable

Related Research

People also read lists articles that other readers of this article have read.

Recommended articles lists articles that we recommend and is powered by our AI driven recommendation engine.

Cited by lists all citing articles based on Crossref citations.
Articles with the Crossref icon will open in a new tab.