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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 194, 2019 - Issue 4-6: Proceedings of the 2018 International Conference on Phosphorus Chemistry, ICPC-22
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Original Articles

Synthesis, phase formation, crystal structure of M0.5(1+x)FexZr2-x(PO4)3 phosphates, M – transition metals in +2 oxidation state

I. O. GlukhovaDepartment of Chemistry, Lobachevsky State University of Niznhi Novgorod, Nizhni Novgorod, Russia; Correspondence[email protected]
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,
E. A. AsabinaDepartment of Chemistry, Lobachevsky State University of Niznhi Novgorod, Nizhni Novgorod, Russia; View further author information
,
V. I. Pet'kovDepartment of Chemistry, Lobachevsky State University of Niznhi Novgorod, Nizhni Novgorod, Russia; View further author information
,
O. V. ButrinaDepartment of Chemistry, Lobachevsky State University of Niznhi Novgorod, Nizhni Novgorod, Russia; View further author information
&
A. M. KovalskyNational University of Science and Technology «MISiS», Moscow, RussiaView further author information
Pages 554-555 | Received 07 Sep 2018, Accepted 01 Oct 2018, Published online: 18 Dec 2018
 
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Abstract

Phosphates M0.5(1+x)FexZr2-x(PO4)3 (M – Ni, Cu, Zn, Mn) of scandium tungstate related structure were synthesized via sol-gel method (including Pechini technique). The samples were characterized by X-ray diffraction, IR spectroscopy, electron microscopy and microprobe analysis. Composition and temperature regions of solid solutions existence in the studied systems were revealed. The Rietveld refinement was implemented for crystal structure of Mn0.65Fe0.3Zr1.7(PO4)3 to be characterized.

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Funding

The reported study was funded by Russian Foundation for Basic Research (RFBR) according to the research projects No. 18-33-00248, 18-29-12063.

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