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Integrated Ferroelectrics
An International Journal
Volume 129, 2011 - Issue 1
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Original Articles

Synthesis of NiAl-HTLcs/ZSM-5 Composite and Its Application in Benzoin Ethyl Ether Reaction

, , &
Pages 18-24 | Received 04 Aug 2010, Accepted 22 Aug 2010, Published online: 17 Oct 2011
 

Abstract

This article describes the synthesis, characterization and application of a novel hydrotalcite/aluminosilicate composite. The composite was prepared by in-suit synthsis of NiAl-HTLcs on the surface of the ZSM-5 and was characterized by X-ray diffraction, Fourier transform infrared, scanning electron microscopy and nitrogen adsorption measurements. The results show that the ZSM-5 phase in the composite was covered by a rough layer of NiAl-HTLcs. The specific surface area of the composite was larger than that of NiAl-HTLcs. When use in benzoin ethyl ether reaction, the composite showed higher reaction rate and better catalytic activities towrad higher conversion of benzaldehyde (56.54%) and selectivity of benzoin ether compounds (100%) in comparasion with the NiAl-HTLcs phase alone.

Acknowledgments

This work was Supported by the Natural Science Foundation of China(50872086) and the Natural Science Foundation of Shanxi Province(2008011018). Here, we’d like to express gratitude to the grant sincerely.

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