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Integrated Ferroelectrics
An International Journal
Volume 154, 2014 - Issue 1: The 12th China International Nanoscience and Technology Symposium, Chengdu (2013)
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Original Article

Synthesis of Monodisperse Silica Microspheres by a Modified Stöber Method

Xue LeiLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China
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Bing YuLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China;Collaborative Innovation Center for Marine Biomass Fibers, Materials and Textiles of Shandong Province, Qingdao University, ChinaCorrespondenceyubing198,@sina.com
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Hai-Lin CongLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China;Collaborative Innovation Center for Marine Biomass Fibers, Materials and Textiles of Shandong Province, Qingdao University, China
,
Chao TianLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China
,
Yue-Zhong WangLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China
,
Qian-Bin WangLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China
&
Chuan-Kuo LiuLaboratory for New Fiber Materials and Modern Textile, Growing Basis for State Key Laboratory, College of Chemical Engineering, Qingdao University, Qingdao266071, China
 show all
Pages 142-146 | Received 15 Jul 2013, Accepted 07 Feb 2014, Published online: 14 May 2014
 
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Abstract

Monodisperse silica microspheres have drawn much attention for having important applications in many areas. In this paper, a series of monodisperse silica (SiO2) microspheres was synthesized successfully using a modified Stöber method in which tetraethyl orthosilicate (TEOS) was continuously supplied into the reaction system by a syringe pump. By changing the supply rate of TEOS, the diameters of the obtained SiO2 microspheres were controlled very well from 1 μm to 3 μm. Detailed characterization of the silica particles was performed using scanning electron microscopy (SEM).

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