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Integrated Ferroelectrics
An International Journal
Volume 201, 2019 - Issue 1
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Articles

A facile method for synthesis of SnS2 with different morphologies by an ambient pressure tetraethylene glycol solution process

Xuerong ZhengKey Laboratory of Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin, China
,
Jing MaoKey Laboratory of Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin, China
,
Jingjing ZhouKey Laboratory of Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin, China
&
Huiming JiKey Laboratory of Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin, ChinaCorrespondence[email protected]
Pages 224-230 | Received 05 Aug 2015, Accepted 03 Feb 2016, Published online: 10 Dec 2019
 
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ABSTRACT

An ambient pressure solution chemical process was used for synthesis of SnS2 nanocrystals with different morphologies such as nanoparticles, nanosheets, nanospheres and so on. The process was conducted by using diethylene glycol as solvent, stannic chloride and thioacetamide as precursors, polyvinylpyrrolidone as capping agent. The influence of synthesized temperature and reducing agent on the morphologies and phases of product were investigated based on XRD, TEM, HRTEM and EDX. Optical properties of SnS2 nanocrystals were characterized. The results showed that pure phase, ultrathin SnS2 nanosheets were prepared with few polyvinylpyrrolidone exited.

Acknowledgement

The authors acknowledge financial support from Research Program of Natural Science Foundation of Hebei Province (Contract No. E2015202295). The authors would also like to express gratitude to prof. Lan Cui and Ms. Yajing Han for their assistance in TEM and EDX analysis, respectively.

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