Thickness measurement of polychlorotrifluoroethylene coating over metallic seal using terahertz time-domain spectroscopy

ABSTRACT

Polychlorotrifluoroethylene is used as a coating material over metallic seals in low-temperature applications to arrest fluid leakage from the impeller side in turbopumps. Typically, polychlorotrifluoroethylene coating is applied on V-type seals, with a thickness ranging from 80 to 130 μm by spraying an emulsion over the substrate followed by heat treatment. An attempt has been made to measure the polychlorotrifluoroethylene coating thickness over V-type seals using terahertz time-domain spectroscopy in reflection geometry, a noncontact, non-invasive NDT method. When the terahertz pulse from a transmitter photo-conductive antenna is incident on the V-type seal, it penetrates through the polychlorotrifluoroethylene coating. It gets reflected from the coating/base coat interface. Here, the reflected echoes from the air-to-polychlorotrifluoroethylene coating interface and polychlorotrifluoroethylene coating to the basecoat interface get overlapped in the time domain as the polychlorotrifluoroethylene coating layer is very thin. The sparse deconvolution technique separates the individual reflected signals and obtains the time delay signals from various interfaces. From the estimation of time delay values, the thickness of the coating has been computed using the refractive index value extracted using terahertz time-domain spectroscopy in transmission mode before the reflection measurements. The obtained thickness values are in close agreement with the coating thickness measured using optical microscopy.

KEYWORDS:

• Polychlorotrifluroethylene
• Thz time-domain spectroscopy
• thickness estimation
• reflection geometry
• seal

Acknowledgments

We would like to thank Shri. Srirangam Siripothu and their team at PCM/VSSC for the support offered in sample preparation.

Disclosure statement

No potential conflict of interest was reported by the author(s).

Data availability statement

The data supporting this study’s findings are available from the corresponding authors upon reasonable request. No third-party data has been used for this research work.

Additional information

Funding

The author(s) reported that there is no funding associated with the work featured in this article.