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Supramolecular Chemistry Volume 19, 2007 - Issue 3
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Original Articles

The Molecular Recognition of Amines with Calix[6]arene: Conclusive X-ray and NMR Evidence for Endo and Exo Complex Formation between Calix[6]arene and Amines

Young Ju Lee Korea Basic Science Institute, Gwangju Center, Gwangju, 500-757, South Korea
,
Ki Deok Park Korea Basic Science Institute, Gwangju Center, Gwangju, 500-757, South Korea
,
Hyoung Min Yeo Department of Chemistry, Chonnam National University, Gwangju, 500-757, South Korea
,
Seung Whan Ko Department of Chemistry, Chonnam National University, Gwangju, 500-757, South Korea
,
Byung Ju Ryu Department of Chemistry, Chonnam National University, Gwangju, 500-757, South Korea
&
Kye Chun Nam Department of Chemistry, Chonnam National University, Gwangju, 500-757, South KoreaCorrespondence[email protected]
Pages 167-173 | Received 23 May 2006, Accepted 09 Jun 2006, Published online: 24 Jul 2007
 
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Abstract

Calix[6]arene formed an endo-complex with piperidine and its inclusion properties were investigated by NMR spectroscopy and X-ray crystallography. Especially, the DOSY spectrum showed that piperidine formed a unique complex with calix[6]arene.

Acknowledgements

The authors are grateful to Professor S. S. Lee and Mr J. B. Suh at Gyeongsang National University and Professor M. S. Lah at Hanyang University for X-ray crystallography analysis. Korea Basic Science Institute, S. Korea is acknowledged for financial support (KBSI-2006-N25053).

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