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Supramolecular Chemistry Volume 26, 2014 - Issue 3-4: Eighth International Symposium of Macrocyclic and Supramolecular Chemistry (ISMSC-8)
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Articles

Synthesis and supramolecular properties of glycoluril tetramer

Marek StanclDepartment of Chemistry and Research Centre for Toxic Compounds in the Environment, Masaryk University, Kamenice 5, 62500Brno, Czech Republic
,
Laura GilbergDepartment of Chemistry and Research Centre for Toxic Compounds in the Environment, Masaryk University, Kamenice 5, 62500Brno, Czech Republic
,
Lukas UstrnulDepartment of Chemistry and Research Centre for Toxic Compounds in the Environment, Masaryk University, Kamenice 5, 62500Brno, Czech Republic
,
Marek NecasDepartment of Chemistry and Research Centre for Toxic Compounds in the Environment, Masaryk University, Kamenice 5, 62500Brno, Czech Republic
&
Vladimir SindelarDepartment of Chemistry and Research Centre for Toxic Compounds in the Environment, Masaryk University, Kamenice 5, 62500Brno, Czech RepublicCorrespondence[email protected]
Pages 168-172 | Received 28 Jun 2013, Accepted 05 Sep 2013, Published online: 14 Oct 2013
 
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Abstract

Synthesis of glycoluril tetramer bearing hydrogen atoms on its convex face and framed by two xylylene units is reported. This tetramer forms dimeric aggregates in the solid state. Host–guest properties of the tetramer with various ammonium and pyridinium guests were determined using 1H NMR spectroscopy. The results were compared with structurally related host molecules.

Acknowledgements

Support for this work was provided by the Czech Science Foundation (P207/10/0695) and the project CETOCOEN (no. CZ.1.05/2.1.00/01.0001) from the European Regional Development Fund. LG thanks the programme of ‘Employment of Newly Graduated Doctors of Science for Scientific Excellence’ (grant number CZ.1.07/2.3.00/30.009) co-financed from European Social Fund and the state budget of the Czech Republic.

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