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Instrumentation Science & Technology Volume 44, 2016 - Issue 5
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Original Articles

Continuous flow time-resolved small-angle x-ray scattering and X-ray absorption spectroscopy

Guang MoBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, ChinaCorrespondence[email protected]
,
Zhonghua WuBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China
,
Quan CaiBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China
,
Zhihong LiBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China
,
Xueqing XingBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China
,
Zhongjun ChenBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China
,
Jiayi WangBeijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China;Academy of Sciences, Graduate University of the Chinese Academy of Sciences, Beijing, China
,
Chenglong WangCollege of Sciences, Tianjin Polytechnic University, Tianjin, China
&
Guanghua LiuCollege of Sciences, Tianjin Polytechnic University, Tianjin, China
 show all
Pages 537-546 | Published online: 22 Mar 2016
 
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ABSTRACT

A continuous flow device to characterize the growth of nanometer particles was assembled. In-situ millisecond or second-order time-resolved small angle x-ray scattering and x-ray absorption spectroscopy was performed using this device at the Beijing Synchrotron Radiation Facility. The time resolution was adjusted from 10 ms to 1.0 s by changing the flow rate of the solution. The temperature was variable from 5–95°C. Custom-designed pulse eliminators were employed to eliminate adverse pump fluctuations and improve the quality of measurements. The system was used to characterize zinc sulfide nanoparticles by small angle x-ray scattering and x-ray absorption spectroscopy.

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