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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 24
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Original Articles

Suzuki–Miyaura Cross‐Coupling of Unprotected Halopurine Nucleosides in Water—Influence of Catalyst and Cosolvent

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Pages 3713-3721 | Received 14 Jan 2006, Published online: 01 Dec 2006
 

Abstract

Reaction conditions for the Suzuki–Miyaura cross‐coupling of unprotected halopurine nucleosides with arylboronic acids in aqueous media were investigated. A series of arylated purine nucleosides was prepared in water without an organic cosolvent, using either Pd(PPh3)4 or Pd(OAc)2/TPPTS as the catalyst.

Acknowledgment

We thank the University of East Anglia for a studentship, the Nuffield Foundation for financial support, and the EPSRC National Mass Spectrometry Service Centre, Swansea, for the recording of mass spectra.

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