Phase-specific high temperature creep behaviour of a pre-rafted Ni-based superalloy studied by X-ray synchrotron diffraction

Abstract

The phase-specific high temperature creep behaviours of the γ and γ′ phases of a rafted Ni-based single crystal superalloy were investigated by a combination of in situ creep experiments and diffraction of high-energy X-ray synchrotron radiation. In situ experiments were performed at constant temperatures in a 930–1125 °C temperature range and under variable applied stress in order to study the material’s response (plastic strain, load transfer) to stress jumps. Using three crystal diffractometry in transmission (Laue) geometry, it was possible to measure the average lattice parameters of both the matrix and the rafts in the [1 0 0] direction at intervals shorter than 300 s. The absolute precision on the measurement of the constrained transverse mismatch (in the rafts’ plane) is better than 10⁻⁵. Plastic strain occurs within the γ corridors as soon as the Von Mises stress exceeds the Orowan stress. The plasticity of the γ′ rafts apparently depends on the transverse stress (i.e. perpendicular to the tensile axis) exceeding a threshold value of 60 MPa.

Keywords:

• nickel base single crystal superalloy
• lattice mismatch
• in situ experiments
• X-ray diffractometry
• creep

Acknowledgements

The authors are grateful to M. Von Zimmermann (BW5 beamline) and to the DESY staff as to Thomas Buslaps and Veijo Honkimäki from ESRF ID15 beamline for their help in the experiments. P. Caron (ONERA) and J.-Y. Guédou (SNECMA) are acknowledged for providing AM1 samples. Our thanks for grants support for travel costs via CALIPSO (EU Support of Access to Synchrotrons/FELs in Europe) and expenses reimbursed by the ESRF.